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ऊर्जा फैलाव एक्स-रे प्रतिदीप्ति स्पेक्ट्रोमीटर (ईडी-एक्सआरएफ)

Energy Dispersive X-Ray Fluorescence Spectrometer (ED-XRF)

Energy Dispersive X-Ray Fluorescence Spectrometer (ED-XRF)

MAKE: Malvern PANalytical

MODEL: Empirian

Capabilities

Specifications:

  • Elemental Analysis technique
  • Analysis Range: Sodium (Na) to Americium (Am).
  • Concentration Range: 100 % to ppm level.
  • X-Ray Source: Ag anode target (15W).
  • Tube Filters: Six, Software selectable (Blank, Cu 300 µm, Cu 500 µm, Al 50 µm, Al 200 µm, Ti 7 µm, Ag 100 µm)
  • Detector: Silicon Drift detector with active area 30 mm2, having resolution ≤ 140 eV @ Mn Kα
  • Ten autosampler positions with spinner, circular sample holders
  • Software: Omnian (standardless) software for qualitative and quantitative analysis.

Sample Preparation Equipment:

  • Vibratory cup mill for fine grinding of powders to 50-micron size.
  • 40-ton motorized Hydraulic press with a Die Set of 35 mm.

Application:

  • Quality assurance through elemental analysis of raw materials like limestone, clays, and final cement products.
  • Rapidly determine the elemental composition in ores, rocks, and minerals for exploration and quality control.
  • Analysis of heavy metals and pollutants in soil, sediments, and airborne particulates.

Sample Requirement

  • Sample Form: Solid, liquid, Powder, Paste.
  • Dust-free flat solid sample.
  • Solid block/pallets of circular shape having a flat diameter from 28 to 50 mm.
  • Samples in powder form should be of a grain size around 50 microns, and preferred to make pellets for a good signal-to-noise ratio.
  • The minimum amount of sample needed to make a pellet is 10 grams. Boric Acid is used as a binding agent for making pellets.
  • Liquid samples can also be analyzed.
  • For quantification, loss on ignition (LOI) and free moisture parameters are needed and provided by the user.
  • Quantification is performed using the Omnian method, a standardless method.
  • Quantification can be provided in oxide form and elemental form, depending on the user's requirement.

Charges

# Academics(Rs)+18% GST Industry(Rs)+18% GST
750/Sample 1250/Sample

Publications

The data will be updated soon once it is received from the CRF Center.

Contact Us

Name: Dr Jayita Sarkar

Designation: Snr Scientific Officer

Phone: 0291 280 1343

Email: jsarkar[at]iitj[dot]ac[dot]in

Name: Dr Saloni Sharma

Designation: Scientific Officer

Phone: 0291 280 1347

Email: saloni[at]iitj[dot]ac[dot]in

Name: Mr. Lalit Mohan

Designation: Junior Assistant

Phone: 0291 280 1344

Email: lalitmohan[at]iitj[dot]ac[dot]in

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